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范玉兰,卢映琼,薛珺,李勋.自动电位滴定法快速测定脐橙叶片中氯含量[J].中国南方果树,2014,43(4):
自动电位滴定法快速测定脐橙叶片中氯含量
Rapid determination of chlorine content in leaf of navel orange by automatic potentiometric titration
投稿时间:2014-03-12  修订日期:2014-05-22
DOI:
中文关键词:  自动电位滴定  脐橙叶片  氯含量
英文关键词:Automatic potentiometric titration  Leaf  Navel orange  Chlorine
基金项目:国家自然科学基金(50968002)
作者单位E-mail
范玉兰 赣南师范学院 yulanfan@sina.com 
卢映琼 赣南师范学院 luyingqin_2008@163.com 
薛珺 赣南师范学院 xuejun8657@foxmail.com 
李勋* 赣南师范学院 gnsylixun@163.com 
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中文摘要:
      建立了一种基于自动电位滴定技术的脐橙叶片中氯含量的快速检测方法。该法采用稀硝酸浸提脐橙叶片中氯,然后用自动电位滴定法快速测定溶液中氯含量,并考察了方法的测定条件、精密度和准确度。该方法的检出限为0.6249mg/L,加标回收率为94.85%~102.96%,相对标准偏差小于3.0%,故该法适于脐橙叶片中氯含量的快速分析。
英文摘要:
       A new method for rapid determination of chlorine content leaf of navel orange was developed. The chlorine in leaf was extracted by dilute nitric acid and determined by automatic potentiometric titration. The determination condition was optimized, and the accuracy and precision of the method were studied. The results showed that the detection limit was 0.6249mg/L, the recovery was 94.85% ~102.96%, and the RSD was within 3.0%. The proposed method has been successfully applied to determine the chlorine content in leaves of navel orange from southern Jiangxi.
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